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Trimethylsulfoxonium iodide
- Name Trimethylsulfoxonium iodide
- CAS 1774-47-6
- Purity 99%
Product Details
Factory Supply industrial standard Trimethylsulfoxonium iodide 1774-47-6 In Stock
- Molecular Formula: C3H9IOS
- Molecular Weight: 220.074
- Appearance/Colour: white to light yellow crystalline powder
- Melting Point: 208-212 °C (dec.)(lit.)
- PSA： 36.28000
- Density: 1.7074 (estimate)
- LogP: -2.62070
Trimethylsulfoxonium iodide(Cas 1774-47-6) Usage
InChI:InChI=1/C3H9OS.HI/c1-5(2,3)4;/h1-3H3;1H/q+1;/p-1
1774-47-6 Relevant articles
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Senoff,C.V. et al.
, p. 3585 - 3589 (1971)
-
Synergism of virtual screening and medicinal chemistry: Identification and optimization of allosteric antagonists of metabotropic glutamate receptor 1
Noeske, Tobias,Trifanova, Dina,Kauss, Valerjans,Renner, Steffen,Parsons, Christopher G.,Schneider, Gisbert,Weil, Tanja
, p. 5708 - 5715 (2009)
We report the identification of novel po...
Synthesis and structure of [Na4(DMSO)15][(I 3)3(I)]. Self-assembly of hexacoordinated sodium
Duarte-Ruiz, Alvaro,Nunez-Dallos, Nelson,Garzon-Tovar, Luis,Wurst, Klaus,Avella-Moreno, Eliseo,Gomez-Baquero, Fernando
, p. 7110 - 7112 (2011)
A new complex with the molecular formula...
Stereoselective Cyclopropanation of (-)-Levoglucosenone Derivatives Using Sulfonium and Sulfoxonium Ylides
Ledingham, Edward T.,Merritt, Christopher J.,Sumby, Christopher J.,Taylor, Michelle K.,Greatrex, Ben W.
, p. 2652 - 2662 (2017)
The synthesis of tri- and tetrasubstitut...
Deuterated antidepressant medicine
-
Paragraph 0009-0010; 0013-014, (2019/01/23)
The invention provides a compound repres...
Preparation method of medetomidine and intermediate thereof
-
Paragraph 0064; 0065; 0066; 0067, (2017/08/28)
The invention relates to a preparation m...
1-[(4-HYDROXYPRIDIN-4-YL) METHYL]PYRIDINE-2(1H)-ONE DERIVATIVES, PREPARATION METHODS AND USES THEREOF
-
Paragraph 0064, (2013/03/28)
Provided are N-[(4-hydroxypiperidin-4-yl...
1774-47-6 Process route
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108-24-7
acetic anhydride
-
-
61272-23-9,130767-77-0,130767-78-1
3-O-(β-D-galactopyranosyl)-D-arabinose
-
-
74-88-4
methyl iodide
-
-
1669-98-3
Ethyl methyl sulfoxide
-
-
100758-68-7
1,3,4-tri-O-acetyl-2,5-di-O-methyl-D-arabinitol
-
-
19285-93-9,19318-49-1,20316-14-7,25665-99-0,53403-07-9,81600-01-3,83290-15-7,103729-41-5,114183-58-3,25521-30-6
1,5-di-O-acetyl-2,3,4,6-tetra-O-methyl-D-galactitol
-
-
19318-22-0,19318-27-5,84885-38-1,84925-47-3,100758-67-6
1,3,5-tri-O-acetyl-2,4-di-O-methyl-D-arabinitol
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1774-47-6
trimethylsulfoxonium iodide
| Conditions | Yield |
|---|---|
|
With
sodium tetrahydroborate; perchloric acid; trimethylsulfoxonium iodide; trifluoroacetic acid;
In
dimethyl sulfoxide;
Product distribution;
Improved methylation analysis; other saccharides;
|
-
-
67-68-5,8070-53-9
dimethyl sulfoxide
-
-
74-88-4
methyl iodide
-
-
1774-47-6
trimethylsulfoxonium iodide
| Conditions | Yield |
|---|---|
|
at 70 ℃;
for 48h;
|
65%
|
|
for 72h;
Reflux;
|
60%
|
|
for 72h;
Reflux;
|
60%
|
|
|
|
|
In
diethyl ether;
|
|
|
Heating;
|
|
|
at 85 ℃;
for 24h;
|
|
|
Reflux;
Inert atmosphere;
|
|
|
for 72h;
|
126 g
|
1774-47-6 Upstream products
-
67-68-5
dimethyl sulfoxide
-
74-88-4
methyl iodide
-
108-24-7
acetic anhydride
-
61272-23-9
3-O-(β-D-galactopyranosyl)-D-arabinose
1774-47-6 Downstream products
-
67-68-5
dimethyl sulfoxide
-
74-88-4
methyl iodide
-
1030-23-5
2-benzoyloxypropiophenone
-
4660-02-0
2-phenylcyclopropane-1-carbonitrile
