Current location:Home > Product Center > 3-(2,2-Dichlorovinyl)-2,2-dimethylcyclopropanecarbonyl chloride
3-(2,2-Dichlorovinyl)-2,2-dimethylcyclopropanecarbonyl chloride
- Name 3-(2,2-Dichlorovinyl)-2,2-dimethylcyclopropanecarbonyl chloride
- CAS 52314-67-7
- Purity 99%
Product Details
Cost-effective and customizable 3-(2,2-Dichlorovinyl)-2,2-dimethylcyclopropanecarbonyl chloride 52314-67-7 for sale
- Molecular Formula: C8H9Cl3O
- Molecular Weight: 227.518
- Vapor Pressure: 0.0341mmHg at 25°C
- Refractive Index: 1.58
- Boiling Point: 242.4 °C at 760 mmHg
- Flash Point: 98.9 °C
- PSA: 17.07000
- Density: 1.424 g/cm3
- LogP: 3.34300
3-(2,2-Dichlorovinyl)-2,2-dimethylcyclopropanecarbonyl chloride(Cas 52314-67-7) Usage
|
Flammability and Explosibility |
Notclassified |
|
Synthesis |
3-(2,2-Dichlorovinyl)-2,2-dimethylcyclopropanecarbonyl chloride can be prepared by Permethric acid and catalyst stirred in toluene with phosgene at 80-90℃ for 1.5h. |
InChI:InChI=1/C8H9Cl3O/c1-8(2)4(3-5(9)10)6(8)7(11)12/h3-4,6H,1-2H3
52314-67-7 Relevant articles
Development of pyrethroid substrates for esterases associated with pyrethroid resistance in the tobacco budworm, Heliothis virescens (F.)
Huang, Huazhang,Ottea, James A.
, p. 6539 - 6545 (2004)
Assays to detect esterases associated wi...
A spectrophotometric assay for pyrethroid-cleaving enzymes in human serum
Butte, Werner,Kemper, Kerstin
, p. 49 - 53 (1999)
A direct continuous spectrophotometric a...
Preparation method of cyanogen chrysanthemum ester insecticide
-
Paragraph 0021; 0025, (2017/08/25)
The invention discloses a preparation me...
Synthesis of new chiral and nonchiral pyrido [3,2-e],[1,3,4] oxadiazine derivatives
Shet,Shelar,Manvi
body text, p. 149 - 156 (2011/01/03)
A chiral series of 6,7-dichloro-3-[3-(2,...
Synthesis and evaluation of a new series of substituted acyl(thio)urea and thiadiazolo [2,3-a] pyrimidine derivatives as potent inhibitors of influenza virus neuraminidase
Sun, Chuanwen,Zhang, Xiaodong,Huang, Hai,Zhou, Pei
, p. 8574 - 8581 (2008/02/07)
A series of substituted acyl(thio)urea a...
Synthesis and biological activity of N′-(substituted pyrimidin-2-yl)-N-dichlorochrysanthemoyl thioureas and their fused heterocyclic compounds
Xue, Sijia,Guo, Yanling,Li, Jingzhi,Ke, Shaoyong,Duan, Liping
, p. 262 - 264 (2007/10/03)
Five N′-(substituted pyrimidin-2-yl)-N-d...
52314-67-7 Process route
-
-
59042-49-8
cis-permethrinic acid
-
-
52314-67-7,60254-21-9,61914-47-4,66182-41-0,66182-42-1,68539-75-3,69831-14-7,76984-70-8,77026-59-6
(+/-)-cis-2-(2,2-dichloroethenyl)-3,3-dimethylcyclopropanecarboxylic acid chloride
| Conditions | Yield |
|---|---|
|
With
thionyl chloride;
Heating;
|
|
|
With
thionyl chloride;
for 14h;
Ambient temperature;
|
|
|
With
thionyl chloride; N,N-dimethyl-formamide;
In
chloroform;
at 40 ℃;
for 3h;
|
|
|
With
thionyl chloride;
In
dichloromethane;
for 4h;
Heating;
|
|
|
With
thionyl chloride;
Heating;
|
|
|
With
thionyl chloride;
In
N,N-dimethyl-formamide;
at 65 ℃;
for 2h;
|
|
|
With
thionyl chloride;
at 50 ℃;
for 4h;
|
|
|
With
thionyl chloride; N,N-dimethyl-formamide;
In
chloroform;
at 60 - 65 ℃;
for 1h;
|
|
|
With
thionyl chloride;
at 65 ℃;
for 1.5h;
|
|
|
With
thionyl chloride;
|
-
-
61898-95-1
cis,trans methyl 2,2-dimethyl-3-(2',2'-dichlorovinyl)-cyclopropanecarboxylate
-
-
52314-67-7,60254-21-9,61914-47-4,66182-41-0,66182-42-1,68539-75-3,69831-14-7,76984-70-8,77026-59-6
(+/-)-cis-2-(2,2-dichloroethenyl)-3,3-dimethylcyclopropanecarboxylic acid chloride
| Conditions | Yield |
|---|---|
|
Multi-step reaction
with
2
steps
1: NaOH / ethanol; H2
O / Heating
2: SOCl2
, DMF / CHCl3
/ 3 h / 40 °C
With
sodium hydroxide; thionyl chloride; N,N-dimethyl-formamide;
In
ethanol; chloroform; water;
|
52314-67-7 Upstream products
-
55701-05-8
3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropanecarboxylic acid
-
52315-07-8
(RS)-α-cyano-3-phenoxybenzyl (1RS,3RS;1RS,3SR)-3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropane carboxylate
-
79-37-8
oxalyl dichloride
-
59609-49-3
ethyl 3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropanecarboxylate
52314-67-7 Downstream products
-
144917-27-1
3-(2,2-Dichloro-vinyl)-2,2-dimethyl-cyclopropanecarboxylic acid dimethoxy-phosphorylmethyl ester
-
52315-07-8
cypermethrine